Because of Industrialization, the Vocs Are Debasing Both Air and Water Bodies Which Are a Reason For Worry Because of Their Wellbeing Dangers. In the Ongoing Year Utilization of Respectable Metal Impetus to Annihilate Vocs on Location Has Picked Up Significance. Anyway Their Cost Stops Their Utilization. We Have Grown Minimal Effort Progress Metal Oxide Impetuses, For Example, Cuo, Co3o4 and Their Composites (Co3o4cuo) to Be Utilized As Oxidation Impetuses For Vocs. the Procedures Utilized Have Been Hydrothermal (Ht), Sol-Gel Auto Burning (Sga), Chemical Combustion (Cc) Thermal Decomposition (Td), For the Creation of High Surface Zone, and Improved Catalytic Movement of Nana Basic Impetuses (In the Scope of 16 Nm to 71 Nm). the Incorporated Impetuses Were Read For the General Oxidation of Formaldehyde By Watery Potassium Dichromate and Individual Impetus, at Moderate Temperatures (20-40Oc). Co3o4 Being Best Has Been Utilized to Catalyze the Oxidation of Oxalic Corrosive and Benzaldehyde Via Airoxygen at Moderate Temperatures (25O-65Oc) and (60Oc) Separately. As No Reagents Were Utilized For the Oxidation of Oxalic Corrosive and Benzaldehyde, the Heterogeneous Nature, Reusability and Recoverability of Co3o4 Impetus Makes the Procedure a Really Green Technology at Lower Costs.